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Last Updated February, 1999
Foreword by William A. Telliard
Preface
Contributors
1 Volatile Organic Compounds(VOCs)
2 Semivolatile/Nonvolatile Organic Comppunds (SVOCs/NVOCs)
3 Metals
4 Radionuclides
5 Water Quality Parameters
Appendices
Index
1 Volatile Organic Compounds (VOCs)
1A Gas Chromatography/Element-Selective Detection
1A.1 Determination of Vinyl Chloride in Ambient Air by GC with Micro-Argon
Ionization Detection
1A.2 Determination of VOCs in Water by Purge-and-Trap and GC with Micro-Argon
Ionization Detection
1A.3 On-Site Estimation of the Total Concentration of VOCs in Soils: A Decision
Tool for Sample Handling
1B Gas Chromatography/Mass Spectrometry
1B.1 Field Determination of VOCs in Soil and Water by Purge-and-Trap
Thermal Desorption GC/MS
1B.2 Determination of VOCs in Fire and Chemical Accidents by Mobile GC/MS
1C Direct Introduction Mass Spectrometry
1C.1 Direct Determination of Total Trihalomethane in Water by Membrane
Introduction Mass Spectrometry (MIMS)
1C.2 Hgh-Speed Field Screening of VOCs in Water by MIMS
1C.3 High-Speed Field Quantitative Analysis of VOCs in Water by MIMS
1C.4 Field Screening of VOCs in Ground Water Using the Hydrosparge VOC
Sensor
1D Microsensor Devices
1D.1 Real-Time Monitoring of Chlorinated VOCs Using a Hand-Portable
Monitor
1D.2 Rapid Determination of VOCs in Air, Water, and Soil by Field-Portable
GC with Surface Acoustic Wave Detection
1D.3 Rapid Determination of VOCs in Air, Water, and Soil by Microchip GC
1E IR/NIR Spectroscopy
1E.1 Determination of VOCs Using a Fiber-Optic Infrared Hazardous Waste
Screening and Identification (HWI) Sensor
1E.2 Monitoring VOCs in Ground Water and Vadose Zone Using a Photoacoustic
Analyzer (New, Jan. 99)
1F Surface-Enhanced Raman Scattering
1F.1 Determination of VOCs Using a Cone Penetrometer-Deployed Solvent
Sensor with a SERS Fiber-Optic Probe
1G Reagent Chemistry
1G.1 Determination of VOCs Using the Dräger Chip Measuring System
1G.2 On-Site Investigation of Contaminated Areas Through Soil Gas Analysis
1G.3 On-Site Measurement of Contaminants in Liquids
2A Gas Chromatography/Element-Selective Detection
2A.1 Determination of Phenols in Water by Solid-Phase Microextraction
(SPME) and GC/FID
2B Gas Chromatography/Mass Spectrometry
2B.1 Determination of Selected Pesticides in Water by SPME and GC/MS
2B.2 Determination of Tetraethyllead in Water by SPME and GC/MS
2B.3 Field Determination of SVOCs in Soil by Thermal Desorption GC/MS
2B.4 SVOCs in Soil by Microwave-Assisted Extraction and GC/MS (New, Sept.
98)
2C Immunoassays
2C.1 Determination of PCBs in Soil by SFE-ELISA
2C.2 Determination of PCBs in Soil and Water by ELISA
2C.3 Determination of Atrazine in Estuarine and Coastal Sea Waters by
SPE-ELISA
2C.4 Determination of Chloropyrifos in Water by ELISA
2C.5 Determination of Sulfonylurea Herbicides in Water by Multianalyte
ELISA
2C.6 Determination of PAHs in Soil and Water by ELISA
2C.7 Determination of Fenitrothion in Estuarine Waters by ELISA
2C.8 Carbaryl in Water Samples by ELISA (New, Sept. 98)
2C.9 1-Naphthol in Water Samples by ELISA (New, Sept. 98)
2C.10 Enzyme Immunoassay for PCDDs and PCDFs (New,
Jan. 99)
2D Reagent Chemistry
2D.1 Colorimetric Determination of Aromatic Compounds in Soil and Water
Using Solvent Extraction and Friedel-Crafts Reaction (Hanby Method)
2D.2 Colorimetric Determination of TNT and RDX in Soil
2D.3 Colorimetric Determination of Pentachlorophenol in Soil and Water (New,
Sept. 98)
2D.4 Coloroimetric Determination of Ammonium Picrate and Picric Acid in Soil
(New, Jan. 99)
2E Fiber-Optic Sensors
2E.1 Determination of TNT and RDX in Soil and Water Using the NRL Fiber-Optic
Biosensor
2E.2 Fiber-Optic Sensor for the Determination of Irgarol 1051 in Seawater
(New, Jan. 99)
3A Potentiometric Stripping Analysis
3A.1 Determination of Copper, Lead, Cadmium, and Zinc in Water Using
a Hand-Held PSA System
3A.2 Screening for Organoarsenicals in Aqueous Environmental Samples by PSA
with Flow Injection
3B X-ray Fluorescence Spectrometry
3B.1 Determination of Metals in Soil by Field-Portable XRF Spectrometry
3B.2 Determination of Metals in Soil by Energy-Dispersive XRF Spectrometry
by XRF Using Fixed-Based and Transportable Instrumentation
3B.3 Determination of Metals in Soil by XRF Spectrometry via Cone Penetrometry
(SCAPS)
3C Immunoassays
3C.1 Determination of Cadmium in Water by ELISA
3D Specialized Applications
3D.1 Field Determination of Cr(VI) in Water with Preconcentration on
Anion-Exchange Membranes or Beads
3D.2 Determination of Metals in Soil and Sediment by Microwave Acid Digestion
and ICP/OES
4A Separation Procedures
4A.1 Radiostrontium Analysis Using Sorbent Disks
4B Gamma-ray Spectrometry
4B.1 In Situ Analysis of Gamma-Ray-Emitting Radionuclides by Borehole
Logging
5A Anions
5A.1 Determination of Nitrate in Aqueous Matrices Using Nitrate Reductase
(New, Sept. 98)
Appendix 1 Procedural Guidelines
A.1A Guidelines for Dynamic Workplans and Field Analytics Appendix
Appendix 2 Useful Data
A.2A Definitions
A.2B EPA Summary of Field Analytical and Site Characterization Technologies
(New, Sept. 98)
Suppliers Appendix
Indexes
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